HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70663545, compound → HCID 70663169, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70663545 | HCID 70663545 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | HCID 70663169 | HCID 70663169 | — |
Reaction Steps
The title compound was prepared in analogy to example 85, intermediate a, from [4-(2-chloro-phenyl)-pyridin-3-yl]-(2-methoxy-ethyl)-carbamic acid tert-butyl ester and using a gradient of n-heptane:EtOAc (100:0 to 0:100) for the chromatographic purification. Colorless oil (72%). MS (ESI): m/z=263.094 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987307B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-37ad8bc86c3745308257c2e87f43dc08 |
| Source note | uspto-grants-2015_03 |