HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorophenylboronic acid → HCID 70663414, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorophenylboronic acid | HCID 2734322 | — |
| Reactant | HCID 70663198 | HCID 70663198 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | HCID 70663414 | HCID 70663414 | — |
Reaction Steps
The title compound was prepared in analogy to example 72, from (4-iodo-pyridin-3-yl)-isopropyl-carbamic acid tert-butyl ester and 2-chlorophenylboronic acid (CAS RN 1679-18-1) and using a gradient of n-heptane:EtOAc (100:0 to 50:50) for the chromatographic purification. Colorless oil (85%). MS (ESI): m/z=347.15 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987307B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-389e4378359f4038a8666acd2695586e |
| Source note | uspto-grants-2015_03 |