HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylphenyl boronic acid → HCID 70663369, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylphenyl boronic acid | HCID 2733267 | — |
| Reactant | HCID 70663578 | HCID 70663578 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | HCID 70663369 | HCID 70663369 | — |
Reaction Steps
The title compound was prepared in analogy to example 72, from 3-(4-iodo-pyridin-3-ylamino)-propionitrile and 2-methylphenylboronic acid (CAS RN 16419-60-6) and using a gradient of heptane:EtOAc (100:0 to 0:100) for the chromatographic purification. Light brown solid (81%). MS (ESI): m/z=238.13 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987307B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-7b37e4da01234c69a60badee943fb918 |
| Source note | uspto-grants-2015_03 |