HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl carbamate → HCID 69402574, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl carbamate | HCID 12136 | — |
| Reactant | Ethyl 3,3,3-trifluoro-2-oxopropanoate | HCID 2737239 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69402574 | HCID 69402574 | — |
Reaction Steps
To a solution of ethyl 3,3,3-trifluoro-2-oxopropanoate (1500 g, 8.82 mol) in dichloromethane (5000 mL) was added benzyl carbamate (1330 g, 8.82 mol). After 2 days, the reaction mixture was filtered to afford ethyl N-[(benzyloxy)carbonyl]-3,3,3-trifluoro-2-hydroxyalaninate. The material was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987456B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-cc64ca67e88647ca887eb7a380f85410 |
| Source note | uspto-grants-2015_03 |