Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diallylamine | HCID 31279 | — |
| Reactant | 3,6-Dioxabicyclo[3.1.0]hexane | HCID 67511 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 117629641 | HCID 117629641 | — |
Reaction Steps
To a solution of 3,4-epoxytetrahydrofuran (57.4 g, 0.67 mol) in ethanol (344 mL) was added diallylamine (194 g, 2.00 mol). The reaction mixture was heated to 75° C. After 2 days, the reaction mixture was cooled and concentrated under reduced pressure to afford trans-4-(diprop-2-en-1-ylamino)tetrahydrofuran-3-ol. The material was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08987456B2 |
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| Source dataset | uspto-grants-2015_03 |
|---|
| ORD ID | ord-305b344a04bb4719bb58a8da6463c86a |
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| Source note | uspto-grants-2015_03 |
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