Ammonia → HCID 131732615, compound

Participants

Reaction Steps

Prepared from the product of Example 65B (100 mg, 0.38 mmol) according to Method H: 1H NMR (300 MHz, methanol-D4) δ ppm 2.08-2.52 (m, 7H), 3.40-3.61 (m, 4H), 3.75-3.90 (m, 3H), 7.54-7.68 (m, 2H), 8.03 (d, J=3.0 Hz, 1H). MS (DCI/NH3) m/z=264/266 (M+H)+. Anal. Calcd. for C14H18ClN3.3.15HCl.1.2H2O: C, 42.01; H, 5.93; N, 10.50. Found: C, 42.29; H, 5.56; N, 10.10.

Provenance & Evidence