HRID878449

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID222

Ammonia gas

H3N

HCID7812

4-Chloroaniline

C6H6ClN

HCID2763184

Ethyl 2-chloro-1,3-oxazole-4-carboxylate

C6H6ClNO3

PRODUCTS

生成物

HCID68804152

未命名化合物

PROCEDURE

实验过程

Prepared from ethyl 2-chlorooxazole-4-carboxylate (83.5 mg, 0.475 mmol) and 4-chloroaniline (60.5 mg, 0.475 mmol) as described in Example 154A: 1H NMR (500 MHz, DMSO-D6) δ ppm 7.37-7.45 (m, 2H), 7.81-7.89 (m, 2H), 8.91 (s, 1H), 10.45 (s, 1H). MS (DCI/NH3) m/z=274 (M+NH4)+.