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HRID878499

反应详情

EQUATION

反应方程式

HRID 878499 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)c1cccc(C)c1
HCID11455

Ethanone, 1-(3-methylphenyl)-

C9H10O

结构：COC(OC)N(C)C
HCID78373

Methanamine, 1,1-dimethoxy-N,N-dimethyl-

C5H13NO2

PRODUCTS

生成物

1
结构：Cc1cccc(C(=O)/C=C/N(C)C)c1
HCID19807213

(2E)-3-(Dimethylamino)-1-(3-methylphenyl)prop-2-en-1-one

C12H15NO

收率 35%

PROCEDURE

实验过程

The title compound was prepared in 35% yield from 1-(3-methylphenyl)ethanone and DMF-DMA according to the procedure for the preparation of Example 12, part A. 1H NMR (400 MHz, CDCl3): δ 2.39 (3H, s), 2.79-3.11 (6H, m), 5.70 (1H, d, J=12.4 Hz), 7.24-7.31 (2H, m), 7.66-7.71 (2H, m), 7.78 (1H, d, J=12.4 Hz).