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HRID878512

反应详情

EQUATION

反应方程式

HRID 878512 的结构方程式

REACTANTS

反应物

2
反应SMILES：COC(OC)N(C)C
HCID78373

Methanamine, 1,1-dimethoxy-N,N-dimethyl-

C5H13NO2

反应SMILES：CC(=O)c1ccc(S(C)(=O)=O)cc1
HCID82529

1-(4-(Methylsulphonyl)phenyl)ethan-1-one

C9H10O3S

PRODUCTS

产物

1
反应SMILES：CN(C)/C=C/C(=O)c1ccc(S(C)(=O)=O)cc1
HCID86725492

未命名化合物

收率 87%

PROCEDURE

实验过程

The title compound was prepared in 87% yield from 1-[4-(methylsulfonyl)phenyl]ethanone and DMF-DMA according to the procedure for the preparation of Example 12, part A. 1H NMR (400 MHz, CDCl3): δ 2.96 (3H, s), 3.06 (3H, s), 3.19 (3H, s), 5.66 (1H, d, J=12 Hz), 7.83 (1H, d, J=12 Hz), 7.96-8.04 (4H, m).