HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Hexanone → HCID 13434190, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Hexanone | HCID 11583 | — |
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 13434190 | HCID 13434190 | 19.3% |
Reaction Steps
A solution of 2-hexanone (2.0 g, 20 mmol) and DMF-DMA (2.4 g, 20 mmol) in DMF (10 mL) was stirred at 100° C. overnight. The reaction mixture was cooled, concentrated, and purified by flash column chromatography (PE/EtOAc=4:1˜2:1) to give the title compound (0.6 g, 19%) as yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987461B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-214bf7638bb24d66ad4df2311a2d5036 |
| Source note | uspto-grants-2015_03 |