HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 84658805, compound → HCID 86725658, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 84658805 | HCID 84658805 | — |
| Reactant | HCID 178510213 | HCID 178510213 | — |
| Product | HCID 86725658 | HCID 86725658 | — |
Reaction Steps
The title compound was prepared from 2-(5-hydroxy-1H-pyrazol-1-yl)pyridine-4-carbonitrile and (3-chloro-4-cyclopropylphenyl)methanol according to the procedure for the preparation of Example 39, part C. 1H NMR (400 MHz, CDCl3): δ 0.68-0.71 (2H, m), 1.01-1.06 (2H, m), 2.16-2.23 (1H, m), 5.17 (2H, s), 5.73 (1H, d, J=2.0 Hz), 6.94 (1H, d, J=8.0 Hz), 7.20 (1H, dd, J=1.6 Hz, 8.0 Hz), 7.40 (1H, dd, J=1.2 Hz, 5.2 Hz), 7.45 (1H, d, J=1.6 Hz), 7.56 (1H, d, J=1.6 Hz), 8.03 (1H, s), 8.71 (1H, d, J=4.8 Hz). [M+H] Calc'd for C19H15ClN4O, 351; Found, 351.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987461B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-1ffc10556dda4535aa59deac19123c9b |
| Source note | uspto-grants-2015_03 |