Phenethylamine → HCID 68010111, compound
Reaction equation
[C:1]([OH:12])(=O)/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[C:13]1([CH2:19][CH2:20][NH2:21])[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[CH2:20]([NH:21][C:1](=[O:12])/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10])[CH2:19][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1Participants
3
Procedure
The same operation as in Example 1-1 or 1-2 was carried out using trans-2-decenoic acid and 2-phenylethaneamine as starting materials to give the aimed compound. Compound 29 was obtained by the purification using silica gel column chromatography.
Sources & evidence
- ORD record
- ord-f6056bd9d2f942e0965626f7898a271d
- Source dataset
- uspto-grants-2015_03
- Patent number
- US08987486B2
Reaction notes
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