HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzoyl chloride → tert-Butyl (4-Chlorobenzoyl)oxycarbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Reactant | tert-butyl N-hydroxycarbamate | HCID 97534 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | tert-Butyl (4-Chlorobenzoyl)oxycarbamate | HCID 23655003 | — |
Reaction Steps
To a solution of tert-butyl hydroxycarbamate (9.76 g, 73.3 mmol) in DCM (120 mL) at 0° C., is added 4-chlorobenzoyl chloride (8.13 mL, 73.3 mmol) followed by the dropwise addition of
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987504B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-7c4cff7d7ff94ee292992348b3cbb040 |
| Source note | uspto-grants-2015_03 |