HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86700409, compound → HCID 86700408, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86700409 | HCID 86700409 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86700408 | HCID 86700408 | — |
Reaction Steps
To a solution of 6-(1-methyl-1H-indazol-5-yl)morpholin-3-one (17.8 mg, 0.077 mmol) in THF was added BH3 in THF (1M, mmol). The resulting mixture was stirred at room temperature for 10 hr. The crude compound was evaporated to dryness and used for the next step without further purification. LCMS-ESI+: calc'd for C12H15N3O: 218.1 (M+H+); found: 218.2 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987250B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-af3458411c5147519def525373ce9cb5 |
| Source note | uspto-grants-2015_03 |