反应详情

To a stirred solution of 2-(1,1-dimethylethyl)-5-[(phenylmethyl)oxy]pyridine, (5.3 g) in ethanol (150 ml) was added 20% Pd(OH)2 (12.3 g) at 25-30 C. The above mixture was purged with hydrogen for 3 h until it had gone to completion by tlc. The reaction mixture was filtered through celite and the filtrate concentrated in vacuo and purified to give the title compound, 3.9 g

1. customThe above mixture was purged with hydrogen for 3 h until it
2. filtrationThe reaction mixture was filtered through celite
3. concentrationthe filtrate concentrated in vacuo
4. custompurified