HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Cyanophenylboronic acid → 2,2'-(6-Oxo-1-(1-phenylethyl)-1,6-dihydropyridazine-4,5-diyl)dibenzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Cyanophenylboronic acid | HCID 2734325 | — |
| Reactant | 4,5-dichloro-2-(1-phenylethyl)pyridazin-3(2H)-one | HCID 68013986 | — |
| Product | 2,2'-(6-Oxo-1-(1-phenylethyl)-1,6-dihydropyridazine-4,5-diyl)dibenzonitrile | HCID 57385631 | 7.4% |
| Product | 3,3'-(6-Oxo-1-(1-phenylethyl)-1,6-dihydropyridazine-4,5-diyl) dibenzonitrile | HCID 57385884 | — |
Reaction Steps
Compound 5 is prepared from intermediate 1a and 3-cyanophenylboronic acid under the conditions described for example 4. The minor product formed (solid) corresponds to compound 4 (yield:7.4%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08993569B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-a72171a545f64f79a8acb4dcdd0adc41 |
| Source note | uspto-grants-2015_03 |