Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 880397Generated: October 30, 2026

Dichloromethane → HCID 59454526, compound

https://huagongshe.com/reaction/880397

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDichloromethaneHCID 6344—
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 46896396HCID 46896396—
ProductHCID 59454526HCID 59454526—

Reaction Steps

Intermediate 1 (0.443 g, 1.65 mmol) was dissolved in DCM (10 mL) and TFA (5.00 mL) was added. The reaction mixture was stirred for 1.5 h, then was concentrated under reduced pressure and dried under vacuum. The crude title compound was used in the next step without purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08993577B2
Source datasetuspto-grants-2015_03
ORD IDord-30fe79f3df534bb6bbd0ef3114b93ce2
Source noteuspto-grants-2015_03