HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 59454526, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 46896396 | HCID 46896396 | — |
| Product | HCID 59454526 | HCID 59454526 | — |
Reaction Steps
Intermediate 1 (0.443 g, 1.65 mmol) was dissolved in DCM (10 mL) and TFA (5.00 mL) was added. The reaction mixture was stirred for 1.5 h, then was concentrated under reduced pressure and dried under vacuum. The crude title compound was used in the next step without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08993577B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-30fe79f3df534bb6bbd0ef3114b93ce2 |
| Source note | uspto-grants-2015_03 |