HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4-methylpyridine → HCID 66914673, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4-methylpyridine | HCID 77248 | — |
| Reactant | 1-(4-Nitrophenyl)piperazine | HCID 80447 | — |
| Solvent | Diglyme | HCID 8150 | — |
| Product | HCID 66914673 | HCID 66914673 | — |
Reaction Steps
From 1-(4-nitro-phenyl)-piperazine and 2-chloro-4-methylpyridine, by heating in diglyme to give 1-(4-methyl-pyridin-2-yl)-4-(4-nitro-phenyl)-piperazine then catalytic hydrogenation over Raney nickel in methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08993574B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-6c7c5d6e45094f809f539ed9c717c82b |
| Source note | uspto-grants-2015_03 |