HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67491524, compound → HCID 67491681, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67491524 | HCID 67491524 | — |
| Reactant | HCID 67491709 | HCID 67491709 | — |
| Product | HCID 67491681 | HCID 67491681 | — |
Reaction Steps
The title compound was prepared by a method analogous to that described for Intermediate 16, using 1-ethyl 5-methyl 3-methoxy-1H-indazole-1,5-dicarboxylate, the regioisomeric product formed in Step 3. +ESI (M+H) 193.1; 1H NMR (400 MHz, DMSO-d6, δ): 12.65 (br. s., 1H), 12.26 (s, 1H), 8.18 (s, 1H), 7.86 (dd, J=8.9, 1.5 Hz, 1H), 7.38 (d, J=8.8 Hz, 1H), 3.99 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08993586B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-05b2bedef7394d68bcc3b3a71685e6ec |
| Source note | uspto-grants-2015_03 |