HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Methylamino)quinoline-6-carboxylic acid → 2-(Methylamino)quinoline-7-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Methylamino)quinoline-6-carboxylic acid | HCID 67491487 | — |
| Reactant | 7-(Ethoxycarbonyl)quinoline 1-oxide | HCID 67491555 | — |
| Product | 2-(Methylamino)quinoline-7-carboxylic acid | HCID 67491517 | — |
Reaction Steps
The title compound was prepared by a method analogous to that described in Steps 3-4 of Intermediate 20, using 7-(ethoxycarbonyl)quinoline 1-oxide. 1H NMR (400 MHz, DMSO-d6, δ): 8.08 (s, 1H), 7.90 (d, 1H), 7.71-7.62 (m, 2H), 7.21 (s, 1H), 6.84 (d, 1H), 2.91 (d, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08993586B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-035a8e60da8c442591cab97c04687667 |
| Source note | uspto-grants-2015_03 |