HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → 5-Benzimidazolecarboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | 3,4-Diaminobenzoic acid | HCID 69263 | — |
| Product | 5-Benzimidazolecarboxylic acid | HCID 459456 | — |
Reaction Steps
3,4-diaminobenzoic acid (5 g, 32 mmol) and formic acid (20 ml) were mixed and refluxed overnight. Formic acid was removed on rotavapour and water added to the residue to obtain the solid. Solid was filtered and dried to obtain the title compound quantitatively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08993612B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-35751864a8ba44259e31706addd54591 |
| Source note | uspto-grants-2015_03 |