反应详情

To a solution of (3-benzyloxy-4-methylphenyl)methanol (1.0 g) in dichloromethane (50 mL) was added manganese dioxide (2.5 g), and this mixture was stirred at room temperature for 2 days. The insoluble material was removed by filtration and this filtrate was concentrated under reduced pressure. This residue was purified by column chromatography on silica gel (eluent: n-hexane/ethyl acetate) to give the title compound (0.39 g)

1. customThe insoluble material was removed by filtration
2. concentrationthis filtrate was concentrated under reduced pressure
3. customThis residue was purified by column chromatography on silica gel (eluent: n-hexane/ethyl acetate)