Lithium Hydroxide → HCID 131732645, compound

Participants

Reaction Conditions

Reaction Steps

To methyl(2E)-4-(dimethylamino)-2-methylbut-2-enoate (238 mg, 1.51 mmol) in tetrahydrofuran (0.95 mL) and water (0.95 mL) was added LiOH (36 mg, 1.5 mmol). The solution was stirred at 40° C. for 4 hours before being frozen and lyophilized to afford a white semi-solid that was taken on to the next step as is. LRMS (ESI) calc'd for C7H13NO2 [M+]+: 144, found 144.

Provenance & Evidence