Potassium Hydroxide → HCID 16679760, compound

Participants

Reaction Conditions

Reaction Steps

First, 5-tert-butylthiomethyl-5-methylhydantoin (5 g, 23 mmol) was mixed with a 73% aqueous potassium hydroxide solution (5.7 g) and toluene (10 ml), and the mixture was heated to 95° C. and stirred for 51 hours. The HPLC analysis of the reaction solution showed the production of the title compound in a reaction yield of 90%.

Provenance & Evidence