HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66629209, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 66629560 | HCID 66629560 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 66629209 | HCID 66629209 | 12.8% |
Reaction Steps
HCl 2N in Et2O was added to tert-butyl (3-methyl-1,2,4-oxadiazol-5-yl)methyl((1S,2S)-2-phenylcyclopropyl)carbamate (35 mg, 0.106 mmol). The Et2O was decanted and the solid was washed twice with 5 mL of Et2O. The solid was dried by vacuum to get (trans)-N-((3-methyl-1,2,4-oxadiazol-5-yl)methyl)-2-phenylcyclopropanamine hydrochloride (14 mg. Yield 12.8%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08993808B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-7f89c4d9dd6f44618bb9cbccf84048cf |
| Source note | uspto-grants-2015_03 |