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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 882582Generated: October 31, 2026

Trifluoroacetic acid → HCID 70980510, compound

https://huagongshe.com/reaction/882582

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 71004159HCID 71004159—
SolventDichloromethaneHCID 6344—
ProductHCID 70980510HCID 70980510—

Reaction Steps

50 mg (154 mmol) of tert-butyl 2-[4-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)-2,2-dimethylbutanoyl]hydrazinecarboxylate were dissolved in 2 ml of dichloromethane, and 0.4 ml of trifluoroacetic acid was added. The reaction mixture was stirred at RT for 30 min and then concentrated. 55.2 mg (93% purity, 99% of theory) of the title compound were obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08992932B2
Source datasetuspto-grants-2015_03
ORD IDord-54ccdffeb88244fc8bb6b5bac6359c8b
Source noteuspto-grants-2015_03