HRID882692

反应详情

EQUATION

反应方程式

HRID 882692 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of the corresponding Ara-C-tetrapeptide-Z-protected (D) (24.7 mg, 0.03 mmol) in methanol containing Pd/C (10% wt/wt) (11.5 mg) was hydrogenated at 25 psi at room temperature for 2 h. The reaction mixture was filtered, and the filtrate was evaporated to dryness, under reduced pressure, to give D (90% yield).

WORKUP

后处理

  1. filtrationThe reaction mixture was filtered
  2. customthe filtrate was evaporated to dryness, under reduced pressure
  3. customto give D (90% yield)