HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 69454122, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 11547014 | HCID 11547014 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 69454122 | HCID 69454122 | — |
Reaction Steps
100 mg of 8-(2-amino-1,1-dimethylethylsulfanyl)-3-methyl-7-(3-methylbut-2-enyl)-1-(2-oxo-2-phenylethyl)-3,7-dihydropurine-2,6-dione were dissolved in 2 ml of ethyl acetate and treated with excess solution of hydrogen chloride in ethyl acetate. After concentration in vacuo at room temperature, the residue was stirred with 5 ml of diisopropyl ether, and the product was filtered off with suction and dried in a vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08236810B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-bd6f2563f2f24a95a7dcde65f01c6e64 |
| Source note | uspto-grants-2012_08 |