HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroethyl isocyanate → HCID 67027666, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroethyl isocyanate | HCID 16035 | — |
| Reactant | 4-Isobutoxyaniline | HCID 5039140 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 67027666 | HCID 67027666 | — |
Reaction Steps
A solution of 2-chloroethyl isocyanate (15 g, 142 mmols) is added dropwise to a solution of 4-isobutoxy phenylamine (20 g, 121 mmols) in diethyl ether (100 mL) and stirred at RT for 1 h. The solid formed is collected by filtration and recrystallisation from ethanol affords the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08236808B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-1c517b78a4964979afa5860a7bc60935 |
| Source note | uspto-grants-2012_08 |