反应详情

4-(2-Pyridinyl)benzaldehyde (2 gm, 11 mmole), and NaBH4 (0.42 gm, 11 mmole) were stirred at room temperature for 2 hr, ethanol was evaporated, residue dissolved in ethyl acetate washed with saturated NaHCO3 solution, and saturated NaCl solution, dried using Na2SO4 and evaporated to produce white solid (1.5 gm, 75%).

1. customethanol was evaporated
2. dissolutionresidue dissolved in ethyl acetate
3. washwashed with saturated NaHCO3 solution, and saturated NaCl solution
4. customdried
5. customevaporated