HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Pyridin-2-ylbenzaldehyde → (4-(Pyridin-2-yl)phenyl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Pyridin-2-ylbenzaldehyde | HCID 1515240 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Product | (4-(Pyridin-2-yl)phenyl)methanol | HCID 1515239 | 75% |
Reaction Steps
4-(2-Pyridinyl)benzaldehyde (2 gm, 11 mmole), and NaBH4 (0.42 gm, 11 mmole) were stirred at room temperature for 2 hr, ethanol was evaporated, residue dissolved in ethyl acetate washed with saturated NaHCO3 solution, and saturated NaCl solution, dried using Na2SO4 and evaporated to produce white solid (1.5 gm, 75%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08236799B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-fc8826a79a524b8e8ea06bacd63c56c4 |
| Source note | uspto-grants-2012_08 |