HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68665588, compound → HCID 16128818, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68665588 | HCID 68665588 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 16128818 | HCID 16128818 | — |
Reaction Steps
A solution of Compound 40A in CH2Cl2 (2 mL) and TFA (1 mL) was stirred at r.t. overnight afterwhich the solvent was removed in vacuo to obtain the desired product (Compound 40) as pale yellow powder (0.036 g). The compound is racemic (i.e. mixture of both enantiomers). The designated “trans” stereochemistry merely describes the relative stereochemistry for the two substituents on the cyclopropane ring. MS (electrospray): mass calculated for C25H26F3NO4, 461.18; m/z found 462 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08236819B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-db54c87a28984040915a8e194ee5c218 |
| Source note | uspto-grants-2012_08 |