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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 883078Generated: October 31, 2026

HCID 68665588, compound → HCID 16128818, compound

https://huagongshe.com/reaction/883078

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68665588HCID 68665588—
SolventDichloromethaneHCID 6344—
SolventTrifluoroacetic acidHCID 6422—
ProductHCID 16128818HCID 16128818—

Reaction Steps

A solution of Compound 40A in CH2Cl2 (2 mL) and TFA (1 mL) was stirred at r.t. overnight afterwhich the solvent was removed in vacuo to obtain the desired product (Compound 40) as pale yellow powder (0.036 g). The compound is racemic (i.e. mixture of both enantiomers). The designated “trans” stereochemistry merely describes the relative stereochemistry for the two substituents on the cyclopropane ring. MS (electrospray): mass calculated for C25H26F3NO4, 461.18; m/z found 462 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08236819B2
Source datasetuspto-grants-2012_08
ORD IDord-db54c87a28984040915a8e194ee5c218
Source noteuspto-grants-2012_08