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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 884025Generated: November 2, 2026

2-Cyclohexen-1-one, 4,4-dimethyl- → Cyclohexanone, 4,4-dimethyl-

https://huagongshe.com/reaction/884025

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Cyclohexen-1-one, 4,4-dimethyl-HCID 136839—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventPentaneHCID 8003—
ProductCyclohexanone, 4,4-dimethyl-HCID 13816698.3%

Reaction Steps

4,4-dimethyl-cyclohexen-1-one (5 g, 40.3 mmol) were placed in a hydrogen reaction vessel and n-pentane (15 ml) was added, and Pd/C (500 mg) was added thereto. The hydrogen reaction vessel was pressurized with hydrogen (25 psi), and the reaction was conducted for 30 minutes. After completing the reaction, the solid like material was filtered through Celite and the filtrate was concentrated in vacuo to give the title compound (5 g, 98%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08236955B2
Source datasetuspto-grants-2012_08
ORD IDord-c652014a0569480ba4a6094d9076f53a
Source noteuspto-grants-2012_08