HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 68524463, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 68524464 | HCID 68524464 | — |
| Catalyst | HCID 178503042 | HCID 178503042 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 68524463 | HCID 68524463 | — |
Reaction Steps
[4-(5-nitropyridin-2-yloxy)phenyl](4-piperonylpiperazin-1-yl)methanone (0.36 g, 0.78 mmol) was dissolved in a mixed solvent consisting of ethanol (5 mL) and THF (5 mL). To the resulting solution was added 5% platinum-carbon (0.06 g), and stirred at room temperature under a hydrogen atmosphere. Two hours later, the 5% platinum-carbon was removed by filtration, and the solvent was evaporated under reduced pressure, to thereby yield 0.32 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08236826B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-b6c0709dd7ff47c98b7219c97339f4da |
| Source note | uspto-grants-2012_08 |