Hydrochloric Acid → HCID 68527505, compound

HRID 884140Notes

Reaction equation

HRID 884140 reaction equation
[F:1][C:2]1[CH:18]=[C:17]([N+:19]([O-:21])=[O:20])[CH:16]=[CH:15][C:3]=1[O:4][C:5]1[CH:10]=[CH:9][C:8]([NH:11]C(=O)C)=[CH:7][CH:6]=1.[ClH:22]>>[ClH:22].[F:1][C:2]1[CH:18]=[C:17]([N+:19]([O-:21])=[O:20])[CH:16]=[CH:15][C:3]=1[O:4][C:5]1[CH:10]=[CH:9][C:8]([NH2:11])=[CH:7][CH:6]=1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 52172793HCID 52172793, compound

Product 1

HCID 68527505HCID 68527505, compound

Procedure

N-[4-(2-fluoro-4-nitrophenoxy)phenyl]-acetamide (1.00 g, 3.45 mmol) was added to 6 M hydrochloric acid (10 mL), and the resulting solution was refluxed for 2 hours. The resulting reaction solution was concentrated under reduced pressure, to thereby yield 0.910 g of the title compound.

Workup

  1. temperaturethe resulting solution was refluxed for 2 hours
  2. customThe resulting reaction solution
  3. concentrationwas concentrated under reduced pressure

Sources & evidence

ORD record
ord-b6b67644fd754b4793ff1249592fe427
Source dataset
uspto-grants-2012_08
Patent number
US08236826B2

Reaction notes

Loading…