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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 885229Generated: October 30, 2026

Sodium borohydride → HCID 58237585, compound

https://huagongshe.com/reaction/885229

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium borohydrideHCID 4311764—
ReactantHCID 58237566HCID 58237566—
SolventMethanolHCID 887—
ProductHCID 58237585HCID 58237585104.6%

Reaction Steps

To [3-(4-fluoro-2-formyl-phenoxy)-phenyl]-acetic acid ethyl ester (0.35 g, 1.1 mmol) in MeOH (20 mL) was added sodium borohydride (0.052 g, 1.4 mmol), and the reaction was stirred for 10 minutes at room temperature. Once no starting material was seen by analytical tlc, the mixture was worked-up to give the desired product (0.35 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08242145B2
Source datasetuspto-grants-2012_08
ORD IDord-0ac423aeb82e4954b96e855fb4a67324
Source noteuspto-grants-2012_08