HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 58237585, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 58237566 | HCID 58237566 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 58237585 | HCID 58237585 | 104.6% |
Reaction Steps
To [3-(4-fluoro-2-formyl-phenoxy)-phenyl]-acetic acid ethyl ester (0.35 g, 1.1 mmol) in MeOH (20 mL) was added sodium borohydride (0.052 g, 1.4 mmol), and the reaction was stirred for 10 minutes at room temperature. Once no starting material was seen by analytical tlc, the mixture was worked-up to give the desired product (0.35 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08242145B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-0ac423aeb82e4954b96e855fb4a67324 |
| Source note | uspto-grants-2012_08 |