HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Ethyl-4,6-dimethylbenzimidazol-1-yl)methyl-10,11-dihydro-5H-dibenzo[b,f]azepine → HCID 178437439, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Ethyl-4,6-dimethylbenzimidazol-1-yl)methyl-10,11-dihydro-5H-dibenzo[b,f]azepine | HCID 69015480 | — |
| Reactant | HCID 178437417 | HCID 178437417 | — |
| Product | HCID 178437439 | HCID 178437439 | — |
Reaction Steps
[step 1] 2-(2-Ethyl-4,6-dimethylbenzimidazol-1-yl)methyl-10,11-dihydro-5H-dibenzo[b,f]azepine (422 mg, 75%) was obtained in the same manner as in step 1 of Example 1, using 2-ethyl-4,6-dimethylbenzimidazole (256 mg, 1.47 mmol), obtained in Reference Example 1, instead of 2-ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08242151B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-5e856ac07ae641f9b047fbafab891967 |
| Source note | uspto-grants-2012_08 |