HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Ethyl-5-methyl-7-trifluoromethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl-10,11-dihydro-5H-dibenzo[b,f]azepine → HCID 178437439, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Ethyl-5-methyl-7-trifluoromethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl-10,11-dihydro-5H-dibenzo[b,f]azepine | HCID 69016874 | — |
| Reactant | HCID 178437489 | HCID 178437489 | — |
| Product | HCID 178437439 | HCID 178437439 | — |
Reaction Steps
[step 1] 2-(2-Ethyl-5-methyl-7-trifluoromethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl-10,11-dihydro-5H-dibenzo[b,f]azepine (153 mg, 50%) was obtained in the same manner as in step 1 of Example 1, using 2-ethyl-5-methyl-7-trifluoromethyl-3H-imidazo[4,5-b]pyridine (160 mg, 0.700 mmol), obtained in Reference Example 3, instead of 2-ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08242151B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-3cba9b9a3315475197280643827fa158 |
| Source note | uspto-grants-2012_08 |