HuagongsheHuagongshe Chemistry Print Report · For research reference only
(E)-2-[3-(2-Ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl-6,11-dihydrodibenzo[b,e]oxepin-11-ylidene]propiononitrile → HCID 178437439, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (E)-2-[3-(2-Ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl-6,11-dihydrodibenzo[b,e]oxepin-11-ylidene]propiononitrile | HCID 69017955 | — |
| Reactant | (E)-2-(3-hydroxymethyl-6,11-dihydrodibenzo[b,e]oxepin-11-ylidene)propiononitrile | HCID 69018194 | — |
| Product | HCID 178437439 | HCID 178437439 | 369.9% |
Reaction Steps
[step 1] (E)-2-[3-(2-Ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl-6,11-dihydrodibenzo[b,e]oxepin-11-ylidene]propiononitrile (168 mg, 27%) was obtained in the same manner as in step 1 of Example 104, using (E)-2-(3-hydroxymethyl-6,11-dihydrodibenzo[b,e]oxepin-11-ylidene)propiononitrile (264 mg, 0.952 mmol) obtained in Reference Example 30 and 2-ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridine (250 mg, 1.43 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08242151B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-e27b572bfb8c4620a16816ebbf03471d |
| Source note | uspto-grants-2012_08 |