HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67246711, compound → HCID 86658314, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67246711 | HCID 67246711 | — |
| Reactant | HCID 86658308 | HCID 86658308 | — |
| Product | HCID 86658314 | HCID 86658314 | 60% |
Reaction Steps
Obtained from Intermediate 85 (0.80 g, 2.7 mmol) by the procedure described in Intermediate 17. Purification by column chromatography with silica gel eluting with ethyl acetate/n-hexane (1:5) gave the title compound (0.48 g, 60%) as oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08242177B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-e1bc41d51d4f4a29b21357ed487a9842 |
| Source note | uspto-grants-2012_08 |