HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11948473, compound → HCID 11948474, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11948473 | HCID 11948473 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 11948474 | HCID 11948474 | 100% |
Reaction Steps
A solution of [[2-(6-methoxy-[1,5]naphthyridin-4-yl)-4,5,6,7-tetrahydro-2H-indazol-5-yl]-(3-oxo-3,4-dihydro-2H-benzo[1,4]thiazin-6-ylmethyl)-amino]-acetic acid tert-butyl ester (5 mg, 0.009 mmol) in 4 M HCl in Et2O (1 mL) was stirred at RT for 3 h. The reaction mixture was concentrated to provide 4.5 mg (100%) of the title compound. MS (ESI): exact mass calculated for C27H26N6O4S, 530.17; m/z found, 531.08 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08242275B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-d768f3bc88024e23b39d6e47f527b2fd |
| Source note | uspto-grants-2012_08 |