HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 75985013, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Cesium acetate | HCID 5152919 | — |
| Reactant | HCID 72820289 | HCID 72820289 | — |
| Catalyst | Tetrabutylammonium Bromide | HCID 74236 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 75985013 | HCID 75985013 | — |
Reaction Steps
29.6 g (0.1 mol) of 5-bromo-1,1,1-trichloro-4-methoxypent-3-en-2-one, 19.1 g of cesium acetate, 5 g of tetrabutylammonium bromide and 8 g of acetic acid were stirred in 300 ml of acetonitrile at 25° C. for 8 h. The precipitate was filtered off and the organic phase was concentrated under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08242313B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-5ffabc4cae3249539d639ab5c2871d7e |
| Source note | uspto-grants-2012_08 |