HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 86650351, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Potassium Acetate | HCID 517044 | — |
| Reactant | 5-bromo-1,1,1-trifluoro-4-methoxypent-3-en-2-one | HCID 5153113 | — |
| Catalyst | Tetrabutylammonium Bromide | HCID 74236 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86650351 | HCID 86650351 | — |
Reaction Steps
24.8 g (0.1 mol) of 5-bromo-1,1,1-trifluoro-4-methoxypent-3-en-2-one, 20 g of potassium acetate, 5 g of tetrabutylammonium bromide and 8 g of acetic acid were stirred in 300 ml of acetonitrile at 40° C. for 20 h. The precipitate was filtered off and the solvent was removed completely under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08242313B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-7f330ea03c0e44b48d5c4db88bd3b0d1 |
| Source note | uspto-grants-2012_08 |