HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 67049858, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 2-Propenoic acid, 3-(4-formylphenyl)- | HCID 98077 | — |
| Reactant | 1-[3-(Hydroxymethyl)phenyl]ethan-1-one | HCID 14995218 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67049858 | HCID 67049858 | 75.2% |
Reaction Steps
A mixture of 1-(3-hydroxymethyl-phenyl)-ethanone (810 mg), 4-formylcinnamic acid (950 mg, 5.4 mmol) and 1.7 M KOH (6.4 ml) in EtOH (40 ml) was stirred at room temperature for 18 h. The resulting precipitate was filtered and washed with EtOH to give 1.25 g of (E)-3-{4-[(E)-3-(3-hydroxymethyl-phenyl)-3-oxo-propenyl]-phenyl}-acrylic acid as its potassium salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08242175B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-c34bc2a467df47f9a1ce65996bb2b68f |
| Source note | uspto-grants-2012_08 |