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HRID886221

反应详情

EQUATION

反应方程式

HRID 886221 的结构方程式

REACTANTS

反应物

2
结构：CC1(C)OB(c2cnn(CCN3CCOCC3)c2)OC1(C)C
HCID17749924

4-{2-[4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl]ethyl}morpholine

C15H26BN3O3

结构：Cc1nc(-c2cn3c(n2)-c2ccc(Br)cc2OCC3)n(C(C)C)n1
HCID58204322

9-Bromo-2-(1-isopropyl-3-methyl-1H-1,2,4-triazol-5-yl)-5,6-dihydrobenzo[f]imidazo[1,2-d][1,4]oxazepine

C17H18BrN5O

PRODUCTS

生成物

1
结构：Cc1nc(-c2cn3c(n2)-c2ccc(-c4cnn(CCN5CCOCC5)c4)cc2OCC3)n(C(C)C)n1
HCID58204873

未命名化合物

PROCEDURE

实验过程

Similarly to as described in General Procedure C, 8-Bromo-2-(2-isopropyl-5-methyl-2H-[1,2,4]triazol-3-yl)-4,5-dihydro-6-oxa-1,3a-diaza-benzo[e]azulene was reacted with 4-(2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl)ethyl)morpholine. Purification of the crude reaction mixture by reverse phase HPLC gave 210. LCMS: 489.2

WORKUP

后处理

  1. customPurification of the crude
  2. customreaction mixture by reverse phase HPLC