HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → N-(Isoquinolin-3-yl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Isoquinolin-3-Amine | HCID 311869 | — |
| Product | N-(Isoquinolin-3-yl)acetamide | HCID 12366594 | — |
Reaction Steps
3-Aminoisoquinoline (495 mg, 3.44 mmol) was stirred in Ac2O (9 mL) at 60° for 16 hours. The mixture was cooled to room temperature and concentrated in vacuo to provide the title compound which was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08247413B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-fc92afb6bdd2453ab5fb523762a690c5 |
| Source note | uspto-grants-2012_08 |