HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethionamide → HCID 22249370, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethionamide | HCID 2761171 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22249370 | HCID 22249370 | — |
Reaction Steps
To a solution of 2-ethyl-4-thiopyridylamide (10 g) in MeOH (250 ml) was added Raney 2800 Nickel (5 g, Aldrich) in one portion. The mixture was stirred at RT for 2 days then at 60° C. for 16 h. The mixture was filtered, concentrated to provide the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08247430B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-32dabe87641849c5ac32f6c75c2c0847 |
| Source note | uspto-grants-2012_08 |