Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 887606Generated: October 31, 2026

HCID 21961440, compound → HCID 67545961, compound

https://huagongshe.com/reaction/887606

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 21961440HCID 21961440—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
ProductHCID 67545961HCID 67545961—

Reaction Steps

A mixture of 2-methyl-5-[1-methyl-1-(4-nitro-phenyl)-ethyl]-[1,3,4]oxadiazole (1.36 g, 5.5 mmol.) and Pd/C (68 mg) in EtOAc (50 mL), was stirred under 1 atm of H2 for 16 h. The resultant was filtered over Celite®, and the filtrate was concentrated to give the titled compound as a pale yellow crystalline. MS: 218 (M+1) calc'd for C12H16N3O—218.12.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08247430B2
Source datasetuspto-grants-2012_08
ORD IDord-8c3a90afbda84339a32f2d901d5d35b4
Source noteuspto-grants-2012_08