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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 887615Generated: October 31, 2026

HCID 68533040, compound → HCID 68910708, compound

https://huagongshe.com/reaction/887615

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68533040HCID 68533040—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 68910708HCID 68910708—

Reaction Steps

4-[1-Methyl-1-(4-nitro-phenyl)-ethyl]-3,6-dihydro-2H-pyridine-1-carboxylic acid ethyl ester was dissolved in EtOH (150 mL) and suspended with Pd/C (10%, 1 g). The reaction flask was equipped with a balloon filled with H2. The hydrogenation was continued for 3 days. The mixture was filtered through a layer of Celite® and concentrated in vacuo to provide the desired compound as a light brown oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08247430B2
Source datasetuspto-grants-2012_08
ORD IDord-26ddee1dd3e140739f5b2d0bdc93368f
Source noteuspto-grants-2012_08