HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 178467197, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Diethyl squarate | HCID 123228 | — |
| Reactant | HCID 178478680 | HCID 178478680 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178467197 | HCID 178467197 | — |
Reaction Steps
2 g of the compound of Example 1 (6.15 mmol) and 0.9 ml of diethyl squarate are stirred at ambient temperature for 2 hours in 15 ml of ethanol. After adding water, the crystals obtained are filtered off and dried in a desiccator to yield the title product in the form of a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08247441B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-fad967879c014c6b8cd024c8ef1aec99 |
| Source note | uspto-grants-2012_08 |